2022年,国家卫生健康委员会发布了《食品安全国家标准 水产品中27种性激素残留量的测定 液相色谱-串联质谱法》(GB 31656.14-2022)。
该标准规定了水产品中27种性激素残留量检测的制样和液相色谱-串联质谱测定方法。
该标准适用于鱼、虾和蟹可食部分中己二烯雌酚、己烯雌酚、雌酮、己烷雌酚、雌二醇、雌三醇、炔雌醇、苯甲酸雌二醇、群勃龙、诺龙、雄烯二酮、勃地酮、睾酮、炔诺酮、美雄酮、甲基睾酮、康力龙、苯丙酸诺龙、丙酸睾酮、孕酮、21α-羟基孕酮、17α-羟基孕酮、甲羟孕酮、醋酸甲地孕酮、醋酸氯地孕酮、醋酸甲羟孕酮和左炔诺孕酮残留量的测定。
百灵威专注食品安全,配套提供标准品、试剂、仪器及耗材,满足专业检测及扩项需求。
| 品名 | CAS | 货号 |
|---|---|---|
| Dienestrol 100 μg/mL in Methanol 己二烯雌酚 | 84-17-3 | DRE-A12598000ME-100 |
| 17a-Ethinylestradiol 100 μg/mL in Methanol/Water 17a-乙炔雌二醇 | 57-63-6 | DRE-A13245100MW-100 |
| 17α-Ethynylestradiol, 98%, reference material 17α-炔雌醇 | 57-63-6 | 963477新 |
| 17-alpha-Hydroxyprogesterone 17-acetate 17α-羟基孕酮-17-醋酸酯 | 302-23-8 | DRE-C14241010 |
| 17α-Hydroxyprogesterone acetate, 98%, reference material 17α-羟基孕酮醋酸酯 | 302-23-8 | 902532 |
| 17-beta-Estradiol 100 μg/mL in Methanol 17β-雌二醇 | 50-28-2 | DRE-A13213100ME-100 |
| β-Estradiol, 99%, reference material β-雌二醇 | 50-28-2 | 945392新 |
| 17-beta-Estradiol 3-benzoate 7-β-安息香酸3-雌二醇 | 50-50-0 | DRE-C13213120 |
| β-Estradiol 3-benzoate, 98%, reference material β-雌二醇-(3-苯甲酸)酯 | 50-50-0 | 963730 |
| 21-Hydroxyprogesterone 100 μg/mL in Methanol/Water 21-羟基孕酮 | 64-85-7 | DRE-A14241050MW-100 |
| Chloromadinone 17-acetate 100 μg/mL in Methanol/Water 醋酸氯地孕酮 | 302-22-7 | DRE-A11418500MW-100 |
| Chlormadinone acetate, 99%, reference material 醋酸氯地孕酮 | 302-22-7 | 936032 |
| Diethylstilbestrol,100 μg/mL in methanol | 56-53-1 | 2801.18-100-ME |
| Diethylstilbestrol, 99%, reference material 己烯雌酚 | 56-53-1 | 933252新 |
| Estriol 100 μg/mL in Methanol 雌三醇 | 50-27-1 | DRE-A13213200ME-100 |
| Estriol, 98.5%, reference material 雌三醇 | 50-27-1 | 949275 |
| Estrone 100 μg/mL in Methanol 雌酮 | 53-16-7 | DRE-A13213230ME-100 |
| Estrone, 99%, reference material 雌酮 | 53-16-7 | 956191新 |
| Hexestrol 100 μg/mL in methanol 己雌酚 | 84-16-2 | DRE-A14202800ME-100 |
| Hexestrol, 98%, reference material 己烷雌酚 | 84-16-2 | 986066 |
| Levonorgestrel 甲基炔酮 | 797-63-7 | DRE-C14629760 |
| Medroxyprogesterone 17-acetate 100 μg/mL in Methanol/Water 甲羟孕酮-17- 醋酸酯 | 71-58-9 | DRE-A14852015MW-100 |
| Medroxyprogesterone acetate, 99%, reference material 醋酸甲羟孕酮酯 | 71-58-9 | 939676 |
| Medroxyprogesterone 甲羟孕酮 | 520-85-4 | DRE-C14852000 |
| Methandrostenolone 美雄酮 | 72-63-9 | DRE-C14993000 |
| Norethisterone 炔诺酮 | 68-22-4 | DRE-C15644950 |
| Norethindrone, 99%, reference material 炔诺酮 | 68-22-4 | 964464新 |
| Progesterone 100 μg/mL in Methanol 黄体酮 | 57-83-0 | DRE-A16342000ME-100 |
| Progesterone, 99%, reference material 黄体酮 | 57-83-0 | 918979新 |
| Testosterone propionate | 57-85-2 | 14528.22-100MG |
| 标准品/雌二醇-13C2同位素 标准品/雌二醇-13C2同位素 | 82938-05-4 | 726742-1mg |
| 标准品/雌酮-D2同位素 标准品/雌酮-D2同位素 | 56588-58-0 | 722266-10mg |
| 标准品/黄体酮-D9同位素 标准品/黄体酮-D9同位素 | 15775-74-3 | 725654-10mg |
| Progesterone-d9, 98%, reference material 孕酮-d9 | 15775-74-3 | 999402 |
| 标准品/甲醇中己烯雌酚-D8同位素 标准品/甲醇中己烯雌酚-D8同位素 | 91318-10-4 | 91357GA |
| 标准品/甲醇中甲羟孕酮-D3同位素 标准品/甲醇中甲羟孕酮-D3同位素 | 162462-69-3 | 91843a |
| 标准品/左炔诺孕酮-D6同位素 标准品/左炔诺孕酮-D6同位素 | / | 726765-10mg |
| 品名 | CAS | 货号 |
|---|---|---|
| C18 SPE Cartridges, bed wt. 500 mg, volume 3 ml, 50 pcs/pack C18 固相萃取小柱 | / | 2471220 |
| Microporous membrane filters, Nylon 66, non-sterile, white, Ф50, 0.22μm, 50 pcs/pack 微孔滤膜 | / | 993699 |
| 品名 | CAS | 货号 |
|---|---|---|
| Acetic acid, 99.5%, for analysis 乙酸 | 64-19-7 | 991956 危化品 |
| Ammonium hydroxide, 25 - 28 wt.% solution of NH3 in water, for analysis 氢氧化铵 | 1336-21-6 | 335213 危化品 |
| Ethyl acetate, 99.9%, ACS/HPLC Certified 乙酸乙酯 | 141-78-6 | 243083 危化品 |
| Methanol, 99.9%, LC-MS 甲醇 | 67-56-1 | 952707 危化品 |
| Methyl tert-butyl ether, 99%, ACS/HPLC Certified 甲基叔丁基醚 | 1634-04-4 | 471256 危化品 |
| n-Hexane, 95%, ACS/HPLC Certified 正己烷 | 110-54-3 | 208930 危化品 |
| Sodium acetate trihydrate, 99%, for analysis 乙酸钠三水合物 | 6131-90-4 | 961379 |